Title |
ᠰᠢᠩᠭᠡᠨ ᠹᠠᠰᠲᠤ ᠦᠩᠭᠡ ᠶᠢᠨ ᠵᠢᠭ᠌ᠰᠠᠯ ᠤᠨ ᠠᠷᠭᠠ ᠪᠠᠷ ᠵᠠᠭᠠᠨ ᠤ ᠬᠠᠮᠠᠷ ᠴᠡᠴᠡᠭ ᠲᠦ ᠬᠢ ᠸᠢᠲ᠋ᠠᠮᠢᠨ ᠤ C᠋ ᠶᠢᠨ ᠠᠭᠤᠯᠤᠭᠳᠠᠴᠠ ᠶᠢ ᠬᠡᠮᠵᠢᠭᠰᠡᠨ ᠨᠢ |
Creator |
ᠭᠦᠢ ᠯᠢᠩ; ᠪᠠᠭᠠᠨᠠ |
Keyword |
ᠵᠠᠭᠠᠨ ᠤ ᠬᠠᠮᠠᠷ ᠴᠡᠴᠡᠭ; ᠸᠢᠲ᠋ᠠᠮᠢᠨ C; HPLC ᠠᠷᠭᠠ |
Abstract |
ᠦᠨᠳᠦᠷ ᠠᠰᠢᠭᠯᠠᠮᠵᠢᠲᠤ ᠰᠢᠩᠭᠡᠨ ᠹᠠᠰᠲᠤ ᠦᠩᠭᠡ ᠶᠢᠨ ᠵᠢᠭ᠌ᠰᠠᠯ (HPLC)᠋ ᠤᠨ ᠠᠷᠭᠠ ᠪᠠᠷ ᠵᠠᠭᠠᠨ ᠤ ᠬᠠᠮᠠᠷ ᠴᠡᠴᠡᠭ ᠲᠦ ᠬᠢ ᠸᠢᠲ᠋ᠠᠮᠢᠨ C ᠋ ᠶᠢᠨ ᠠᠭᠤᠯᠤᠭᠳᠠᠴᠠ ᠶᠢ ᠬᠡᠮᠵᠢᠬᠦ ᠲᠤᠬᠢᠷᠠᠮᠵᠢᠲᠠᠢ ᠠᠷᠭᠠ ᠶᠢ ᠡᠷᠢᠯᠬᠢᠯᠡᠨᠡ᠃ ᠠᠷᠭᠠ᠄ Hypersil - C18(150mm×4.6,5μm) ᠦᠩᠭᠡ ᠶᠢᠨ ᠵᠢᠭ᠌ᠰᠠᠯ ᠤᠨ ᠪᠠᠭᠠᠨᠠ ᠶᠢ ᠬᠡᠷᠡᠭᠯᠡᠵᠦ᠂ pH=6.0 ᠋ ᠤᠨ 0.30mo/L ᠹᠤᠰᠹᠤᠷ ᠬᠦᠴᠢᠯ ᠦᠨ ᠬᠤᠶᠠᠷ ᠤᠰᠤᠳᠦ᠋ᠷᠦᠭᠴᠢᠲᠦ ᠺᠠᠯᠼ᠄ ᠡᠲ᠋ᠢᠯ ᠨᠢᠲ᠋ᠷᠢᠯ (90᠄ 10)᠋ ᠢᠶᠠᠷ ᠤᠷᠤᠰᠤᠮᠠᠯ ᠹᠠᠰ ᠪᠤᠯᠭᠠᠨᠠ᠃ ᠬᠡᠷᠡᠭᠯᠡᠬᠦ ᠡᠴᠡ ᠪᠡᠨ ᠡᠮᠦᠨᠡ ᠵᠢᠵᠢᠭ᠌ ᠭᠤᠤᠷᠰᠤᠲᠤ ᠱᠦᠭᠦᠯᠲᠡ (ᠰᠢᠭᠦᠯᠲᠡ)᠋ ᠶᠢᠨ ᠰᠢᠰᠲ᠋ᠧᠮ ᠢᠶᠡᠷ ᠦᠩᠭᠡᠷᠡᠭᠦᠯᠦᠨᠡ᠃ ᠬᠡᠮᠵᠢᠯᠲᠡ ᠶᠢᠨ ᠳᠤᠯᠭᠢᠶᠠᠨ ᠤ ᠤᠷᠲᠤ ᠨᠢ 254nm᠂ ᠪᠠᠭᠠᠨᠠ ᠶᠢᠨ ᠲᠤᠯᠭᠠᠴᠠ ᠨᠢ 25℃᠂ ᠤᠷᠤᠰᠬᠠᠬᠤ ᠬᠤᠷᠳᠤᠴᠠ ᠨᠢ 0.60ml/min᠃ ᠦᠷᠡ ᠳ᠋ᠦᠩ᠄ ᠸᠢᠲ᠋ᠠᠮᠢᠨ C ᠨᠢ 0.20~1.00ug᠋᠋ ᠤᠨ ᠬᠡᠪᠴᠢᠶᠡᠨ ᠳᠤᠲᠤᠷᠠ ᠣᠷᠭᠢᠯ ᠤᠨ ᠲᠠᠯᠠᠪᠠᠢ ᠲᠠᠢ ᠪᠠᠨ ᠮᠠᠰᠢ ᠰᠠᠢ᠌ᠨ ᠱᠤᠭᠤᠮᠯᠢᠭ ᠬᠠᠷᠢᠴᠠᠭᠠ ᠲᠠᠢ (γ=0.9999) ᠪᠠᠢ᠌ᠵᠤ᠂ ᠦᠯᠢᠭᠡᠷ ᠨᠡᠮᠡᠵᠦ ᠪᠤᠴᠠᠭᠠᠨ ᠠᠪᠬᠤ ᠲᠤᠷᠰᠢᠯᠲᠠ ᠶᠢᠨ ᠳᠤᠮᠳᠠᠴᠢ ᠪᠤᠴᠠᠭᠠᠮᠵᠢ ᠨᠢ 96.4%᠂ RSD=1.36% ᠪᠤᠢ᠃ ᠳ᠋ᠦᠩᠨᠡᠯᠲᠡ᠄ ᠲᠤᠰ ᠠᠷᠭᠠ ᠨᠢ ᠬᠡᠷᠡᠭᠯᠡᠬᠦ ᠳᠦ ᠳᠦᠭᠦᠮ ᠪᠦᠭᠡᠳ ᠨᠠᠢ᠌ᠳᠠᠪᠤᠷᠢᠲᠠᠢ᠂ ᠣᠨᠣᠪᠴᠢᠲᠤ ᠴᠢᠨᠠᠷ ᠢᠶᠠᠷ ᠰᠠᠢ᠌ᠨ ᠪᠤᠯᠬᠤᠷ ᠵᠠᠭᠠᠨ ᠤ ᠬᠠᠮᠠᠷ ᠴᠡᠴᠡᠭ ᠦᠨ ᠴᠢᠨᠠᠷ ᠤᠨ ᠪᠠᠷᠢᠮᠵᠢᠶᠠ ᠶᠢ ᠲᠤᠭᠲᠠᠭᠠᠬᠤ ᠰᠤᠳᠤᠯᠭᠠᠨ ᠳᠤ ᠬᠡᠷᠡᠭᠯᠡᠵᠦ ᠪᠤᠯᠤᠨᠠ᠃ |
Original Literature |
View Original Paper
|
出自 |
内蒙古民族大学学报(蒙医药学)
2013年
第1期
|